Profiling of 2-Acetyl-1-Pyrroline and Other Volatile Compounds in Raw and Cooked Rice of Traditional and Improved Varieties of India

Herein, optimized headspace solid phase microextraction with gas chromatography–tandem mass spectrometry (HS-SPME-GC-MS/MS) was used to estimate the 2-acetyl-1-pyrroline (2-AP) in raw and cooked rice samples of ten different traditional and improved varieties. Furthermore, HS-SPME-GC-MS-based volati...

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Autores principales: Kasote, Deepak, Singh, Vivek Kumar, Bollinedi, Haritha, Singh, Ashok Kumar, Sreenivasulu, Nese, Regina, Ahmed
Formato: Journal Article
Lenguaje:Inglés
Publicado: MDPI 2021
Materias:
Acceso en línea:https://hdl.handle.net/10568/164213
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author Kasote, Deepak
Singh, Vivek Kumar
Bollinedi, Haritha
Singh, Ashok Kumar
Sreenivasulu, Nese
Regina, Ahmed
author_browse Bollinedi, Haritha
Kasote, Deepak
Regina, Ahmed
Singh, Ashok Kumar
Singh, Vivek Kumar
Sreenivasulu, Nese
author_facet Kasote, Deepak
Singh, Vivek Kumar
Bollinedi, Haritha
Singh, Ashok Kumar
Sreenivasulu, Nese
Regina, Ahmed
author_sort Kasote, Deepak
collection Repository of Agricultural Research Outputs (CGSpace)
description Herein, optimized headspace solid phase microextraction with gas chromatography–tandem mass spectrometry (HS-SPME-GC-MS/MS) was used to estimate the 2-acetyl-1-pyrroline (2-AP) in raw and cooked rice samples of ten different traditional and improved varieties. Furthermore, HS-SPME-GC-MS-based volatile profiling was subjected to untargeted analyses to identify major odorants in raw and cooked rice samples, and to understand chemical proximities among volatile profiles. Results showed that 2-AP content was remarkably increased in cooked rice compared to raw. Among the varieties studied, Pusa-1652 (Improved Kala Namak) and Kala Namak-2 were superior in the 2-AP content than Basmati varieties. Additionally, Govind Bhog, Kala Jeera and Jeera-32 had 2-AP content equivalent to or superior to Basmati rice varieties. Altogether, 18 and 22 volatiles were identified in the raw and cooked rice samples studied, respectively. Of these, ethyl butyrate, ethyl 3-methylbutanoate, 2-undecanone, ethyl benzoate, ethyl benzeneacetate, 2-methylnaphthalene, and 1-methylnaphthalene were characteristically detected in the cooked rice. The high amount of 2-ethyl-1-hexanol was uniquely found in raw rice samples, which can be a marker compound for freshly milled rice. Along with 2-AP, butanoic acid and benzoic acid derivatives, phenylethyl alcohol, ethyl 3-hydroxybutyrate, and indole may be responsible for the overall perceived characteristic Basmati-like aroma in cooked rice.
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spelling CGSpace1642132025-12-08T09:54:28Z Profiling of 2-Acetyl-1-Pyrroline and Other Volatile Compounds in Raw and Cooked Rice of Traditional and Improved Varieties of India Kasote, Deepak Singh, Vivek Kumar Bollinedi, Haritha Singh, Ashok Kumar Sreenivasulu, Nese Regina, Ahmed plant science health professions (miscellaneous) health(social science) microbiology food science Herein, optimized headspace solid phase microextraction with gas chromatography–tandem mass spectrometry (HS-SPME-GC-MS/MS) was used to estimate the 2-acetyl-1-pyrroline (2-AP) in raw and cooked rice samples of ten different traditional and improved varieties. Furthermore, HS-SPME-GC-MS-based volatile profiling was subjected to untargeted analyses to identify major odorants in raw and cooked rice samples, and to understand chemical proximities among volatile profiles. Results showed that 2-AP content was remarkably increased in cooked rice compared to raw. Among the varieties studied, Pusa-1652 (Improved Kala Namak) and Kala Namak-2 were superior in the 2-AP content than Basmati varieties. Additionally, Govind Bhog, Kala Jeera and Jeera-32 had 2-AP content equivalent to or superior to Basmati rice varieties. Altogether, 18 and 22 volatiles were identified in the raw and cooked rice samples studied, respectively. Of these, ethyl butyrate, ethyl 3-methylbutanoate, 2-undecanone, ethyl benzoate, ethyl benzeneacetate, 2-methylnaphthalene, and 1-methylnaphthalene were characteristically detected in the cooked rice. The high amount of 2-ethyl-1-hexanol was uniquely found in raw rice samples, which can be a marker compound for freshly milled rice. Along with 2-AP, butanoic acid and benzoic acid derivatives, phenylethyl alcohol, ethyl 3-hydroxybutyrate, and indole may be responsible for the overall perceived characteristic Basmati-like aroma in cooked rice. 2021-08-18 2024-12-19T12:53:36Z 2024-12-19T12:53:36Z Journal Article https://hdl.handle.net/10568/164213 en Open Access MDPI Kasote, Deepak; Singh, Vivek Kumar; Bollinedi, Haritha; Singh, Ashok Kumar; Sreenivasulu, Nese and Regina, Ahmed. 2021. Profiling of 2-Acetyl-1-Pyrroline and Other Volatile Compounds in Raw and Cooked Rice of Traditional and Improved Varieties of India. Foods, Volume 10 no. 8 p. 1917
spellingShingle plant science
health professions (miscellaneous)
health(social science)
microbiology
food science
Kasote, Deepak
Singh, Vivek Kumar
Bollinedi, Haritha
Singh, Ashok Kumar
Sreenivasulu, Nese
Regina, Ahmed
Profiling of 2-Acetyl-1-Pyrroline and Other Volatile Compounds in Raw and Cooked Rice of Traditional and Improved Varieties of India
title Profiling of 2-Acetyl-1-Pyrroline and Other Volatile Compounds in Raw and Cooked Rice of Traditional and Improved Varieties of India
title_full Profiling of 2-Acetyl-1-Pyrroline and Other Volatile Compounds in Raw and Cooked Rice of Traditional and Improved Varieties of India
title_fullStr Profiling of 2-Acetyl-1-Pyrroline and Other Volatile Compounds in Raw and Cooked Rice of Traditional and Improved Varieties of India
title_full_unstemmed Profiling of 2-Acetyl-1-Pyrroline and Other Volatile Compounds in Raw and Cooked Rice of Traditional and Improved Varieties of India
title_short Profiling of 2-Acetyl-1-Pyrroline and Other Volatile Compounds in Raw and Cooked Rice of Traditional and Improved Varieties of India
title_sort profiling of 2 acetyl 1 pyrroline and other volatile compounds in raw and cooked rice of traditional and improved varieties of india
topic plant science
health professions (miscellaneous)
health(social science)
microbiology
food science
url https://hdl.handle.net/10568/164213
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