13CNMR assignments for methyls and quarternary carbons of the limonoid abacunone
The high field1H and13C resonances of obacunone were established by a series of I D and 2D NMR experiments. The13C-NMR signals of the five tertiary methyl groups and all quatenary carbons were unambiguously assigned. The results confirm the stereochemical assignments at all stereogenic centres.
| Main Authors: | , , , , |
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| Format: | Journal Article |
| Language: | Inglés |
| Published: |
1996
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| Subjects: | |
| Online Access: | https://hdl.handle.net/10568/103255 |
| Summary: | The high field1H and13C resonances of obacunone were established by a series of I D and 2D NMR experiments. The13C-NMR signals of the five tertiary methyl groups and all quatenary carbons were unambiguously assigned. The results confirm the stereochemical assignments at all stereogenic centres. |
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