Enhancing Organic Selenium Forms in Alfalfa Forage Through Inorganic Selenium Foliar Application: Insights from Laboratory and Field Studies Using X-Ray Spectroscopy

Selenium (Se) is an essential micronutrient, yet its deficiency remains a global concern. This study investigates the biofortification of alfalfa (Medicago sativa cv. ProINTA Super Monarca GR9) via foliar Se application to enhance Se accumulation and transformation into bioavailable organic forms. A...

Descripción completa

Detalles Bibliográficos
Autores principales: Sánchez-Martín, María Jesús, Gaggiotti, Monica Del Carmen, Simonelli, Laura, Marini, Carlo, Marini, Federico, Boada, Roberto, Llugany, Mercè, Valiente, Manuel, Céccoli, Gabriel, Stoffel, María Micaela, Viltres-Portales, Marcia, Picco, Juan Manuel, Guevara, María Gabriela, Muñoz, Fernando Felipe
Formato: info:ar-repo/semantics/artículo
Lenguaje:Inglés
Publicado: MDPI 2025
Materias:
Acceso en línea:http://hdl.handle.net/20.500.12123/21517
https://www.mdpi.com/2073-4395/15/3/580
https://doi.org/10.3390/agronomy15030580
_version_ 1855038414170095616
author Sánchez-Martín, María Jesús
Gaggiotti, Monica Del Carmen
Simonelli, Laura
Marini, Carlo
Marini, Federico
Boada, Roberto
Llugany, Mercè
Valiente, Manuel
Céccoli, Gabriel
Stoffel, María Micaela
Viltres-Portales, Marcia
Picco, Juan Manuel
Guevara, María Gabriela
Muñoz, Fernando Felipe
author_browse Boada, Roberto
Céccoli, Gabriel
Gaggiotti, Monica Del Carmen
Guevara, María Gabriela
Llugany, Mercè
Marini, Carlo
Marini, Federico
Muñoz, Fernando Felipe
Picco, Juan Manuel
Simonelli, Laura
Stoffel, María Micaela
Sánchez-Martín, María Jesús
Valiente, Manuel
Viltres-Portales, Marcia
author_facet Sánchez-Martín, María Jesús
Gaggiotti, Monica Del Carmen
Simonelli, Laura
Marini, Carlo
Marini, Federico
Boada, Roberto
Llugany, Mercè
Valiente, Manuel
Céccoli, Gabriel
Stoffel, María Micaela
Viltres-Portales, Marcia
Picco, Juan Manuel
Guevara, María Gabriela
Muñoz, Fernando Felipe
author_sort Sánchez-Martín, María Jesús
collection INTA Digital
description Selenium (Se) is an essential micronutrient, yet its deficiency remains a global concern. This study investigates the biofortification of alfalfa (Medicago sativa cv. ProINTA Super Monarca GR9) via foliar Se application to enhance Se accumulation and transformation into bioavailable organic forms. A controlled environment experiment in a plant growth chamber and a one-season open-field trial (January 2023, Argentina) were conducted. Treatments included sodium selenate (Se(VI)), sodium selenite (Se(IV)), and a 1:1 mixture, applied at 45 and 90 g Se ha−1, with and without the biostimulant BIOFORGE®. Treated plants exhibited increased Se content, correlating with the applied doses. X-ray absorption spectroscopy (XAS) confirmed that most inorganic Se was transformed into organic Se forms, with Se(IV) treatments yielding the highest concentrations of organic Se species such as selenocysteine (SeCys) and selenomethionine (SeMet). Open-field trials showed a complete conversion of Se, though total Se accumulation was lower than in controlled conditions. Se treatments did not affect forage quality or biomass production. The biostimulant slightly reduced Se uptake but did not compromise biofortification. These results highlight Se(IV) as the optimal treatment for alfalfa biofortification, presenting a sustainable strategy to enhance dietary Se intake through functional foods.
format info:ar-repo/semantics/artículo
id INTA21517
institution Instituto Nacional de Tecnología Agropecuaria (INTA -Argentina)
language Inglés
publishDate 2025
publishDateRange 2025
publishDateSort 2025
publisher MDPI
publisherStr MDPI
record_format dspace
spelling INTA215172025-02-28T13:52:18Z Enhancing Organic Selenium Forms in Alfalfa Forage Through Inorganic Selenium Foliar Application: Insights from Laboratory and Field Studies Using X-Ray Spectroscopy Sánchez-Martín, María Jesús Gaggiotti, Monica Del Carmen Simonelli, Laura Marini, Carlo Marini, Federico Boada, Roberto Llugany, Mercè Valiente, Manuel Céccoli, Gabriel Stoffel, María Micaela Viltres-Portales, Marcia Picco, Juan Manuel Guevara, María Gabriela Muñoz, Fernando Felipe Selenio Experimentación en Laboratorio Experimentación en Campo Espectros Copia de Rayos X Espectroscopia Selenium Medicago sativa Laboratory Experimentation Field Experimentation X-ray Spectroscopy Spectroscopy Alfalfa Lucerne Selenium (Se) is an essential micronutrient, yet its deficiency remains a global concern. This study investigates the biofortification of alfalfa (Medicago sativa cv. ProINTA Super Monarca GR9) via foliar Se application to enhance Se accumulation and transformation into bioavailable organic forms. A controlled environment experiment in a plant growth chamber and a one-season open-field trial (January 2023, Argentina) were conducted. Treatments included sodium selenate (Se(VI)), sodium selenite (Se(IV)), and a 1:1 mixture, applied at 45 and 90 g Se ha−1, with and without the biostimulant BIOFORGE®. Treated plants exhibited increased Se content, correlating with the applied doses. X-ray absorption spectroscopy (XAS) confirmed that most inorganic Se was transformed into organic Se forms, with Se(IV) treatments yielding the highest concentrations of organic Se species such as selenocysteine (SeCys) and selenomethionine (SeMet). Open-field trials showed a complete conversion of Se, though total Se accumulation was lower than in controlled conditions. Se treatments did not affect forage quality or biomass production. The biostimulant slightly reduced Se uptake but did not compromise biofortification. These results highlight Se(IV) as the optimal treatment for alfalfa biofortification, presenting a sustainable strategy to enhance dietary Se intake through functional foods. EEA Rafaela Fil: Sánchez-Martín, María Jesús. Universitat Autònoma de Barcelona. Faculty of Science. Department of Chemistry. GTS Research Group; España Fil: Gaggiotti, Monica Del Carmen. Instituto Nacional de Tecnología Agropecuaria (INTA). Estación Experimental Agropecuaria Rafaela. Instituto de Investigación de la Cadena Láctea (IDICAL); Argentina Fil: Gaggiotti, Monica Del Carmen. Consejo Nacional de Investigaciones Científicas y Técnicas. Instituto de Investigación de la Cadena Láctea (IDICAL); Argentina Fil: Simonelli, Laura. ALBA Synchrotron; España Fil: Marini, Carlo. ALBA Synchrotron; España Fil: Marini, Federico. Sapienza University of Rome. Department of Chemistry; Italia Fil: Boada, Roberto. Universitat Autònoma de Barcelona. Faculty of Science. Department of Chemistry. GTS Research Group; España Fil: Llugany, Mercè. Universitat Autonòma de Barcelona. Faculty of Biosciences. Plant Physiology Group (BABVE); España Fil: Valiente, Manuel. Universitat Autònoma de Barcelona. Faculty of Science. Department of Chemistry. GTS Research Group; España Fil: Céccoli, Gabriel. Universidad Nacional del Litoral. Facultad de Ciencias Agrarias. Cátedra de Fisiología Vegetal; Argentina Fil: Céccoli, Gabriel. Consejo Nacional de Investigaciones Científicas y Técnicas. Instituto de Ciencias Agropecuarias del Litoral (ICiAgro); Argentina Fil: Céccoli, Gabriel. Universidad Nacional del Litoral. Facultad de Ciencias Agrarias. Instituto de Ciencias Agropecuarias del Litoral (ICiAgro); Argentina Fil: Stoffel, María Micaela. Universidad Nacional del Litoral. Facultad de Ciencias Agrarias. Cátedra de Fisiología Vegetal; Argentina Fil: Viltres-Portales, Marcia. Universitat Autònoma de Barcelona. Faculty of Science. Department of Chemistry. GTS Research Group; España Fil: Picco, Juan Manuel. Instituto Nacional de Tecnología Agropecuaria (INTA). Estación Experimental Agropecuaria Rafaela; Argentina Fil: Guevara, María Gabriela. Universidad Nacional de Mar del Plata. Instituto de Investigaciones Biológicas (IIB); Argentina Fil: Guevara, María Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas. Instituto de Investigaciones Biológicas (IIB); Argentina Fil: Muñoz, Fernando Felipe. Universidad Nacional del Litoral. Facultad de Ciencias Agrarias. Cátedra de Fisiología Vegetal; Argentina Fil: Muñoz, Fernando Felipe. Universidad Nacional de Mar del Plata. Instituto de Investigaciones Biológicas (IIB); Argentina Fil: Muñoz, Fernando Felipe. Consejo Nacional de Investigaciones Científicas y Técnicas. Instituto de Investigaciones Biológicas (IIB); Argentina 2025-02-28T13:48:58Z 2025-02-28T13:48:58Z 2025-02 info:ar-repo/semantics/artículo info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion http://hdl.handle.net/20.500.12123/21517 https://www.mdpi.com/2073-4395/15/3/580 2073-4395 https://doi.org/10.3390/agronomy15030580 eng info:eu-repo/semantics/openAccess http://creativecommons.org/licenses/by-nc-sa/4.0/ Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International (CC BY-NC-SA 4.0) application/pdf MDPI Agronomy 15 (3) : 580. (February 2025)
spellingShingle Selenio
Experimentación en Laboratorio
Experimentación en Campo
Espectros Copia de Rayos X
Espectroscopia
Selenium
Medicago sativa
Laboratory Experimentation
Field Experimentation
X-ray Spectroscopy
Spectroscopy
Alfalfa
Lucerne
Sánchez-Martín, María Jesús
Gaggiotti, Monica Del Carmen
Simonelli, Laura
Marini, Carlo
Marini, Federico
Boada, Roberto
Llugany, Mercè
Valiente, Manuel
Céccoli, Gabriel
Stoffel, María Micaela
Viltres-Portales, Marcia
Picco, Juan Manuel
Guevara, María Gabriela
Muñoz, Fernando Felipe
Enhancing Organic Selenium Forms in Alfalfa Forage Through Inorganic Selenium Foliar Application: Insights from Laboratory and Field Studies Using X-Ray Spectroscopy
title Enhancing Organic Selenium Forms in Alfalfa Forage Through Inorganic Selenium Foliar Application: Insights from Laboratory and Field Studies Using X-Ray Spectroscopy
title_full Enhancing Organic Selenium Forms in Alfalfa Forage Through Inorganic Selenium Foliar Application: Insights from Laboratory and Field Studies Using X-Ray Spectroscopy
title_fullStr Enhancing Organic Selenium Forms in Alfalfa Forage Through Inorganic Selenium Foliar Application: Insights from Laboratory and Field Studies Using X-Ray Spectroscopy
title_full_unstemmed Enhancing Organic Selenium Forms in Alfalfa Forage Through Inorganic Selenium Foliar Application: Insights from Laboratory and Field Studies Using X-Ray Spectroscopy
title_short Enhancing Organic Selenium Forms in Alfalfa Forage Through Inorganic Selenium Foliar Application: Insights from Laboratory and Field Studies Using X-Ray Spectroscopy
title_sort enhancing organic selenium forms in alfalfa forage through inorganic selenium foliar application insights from laboratory and field studies using x ray spectroscopy
topic Selenio
Experimentación en Laboratorio
Experimentación en Campo
Espectros Copia de Rayos X
Espectroscopia
Selenium
Medicago sativa
Laboratory Experimentation
Field Experimentation
X-ray Spectroscopy
Spectroscopy
Alfalfa
Lucerne
url http://hdl.handle.net/20.500.12123/21517
https://www.mdpi.com/2073-4395/15/3/580
https://doi.org/10.3390/agronomy15030580
work_keys_str_mv AT sanchezmartinmariajesus enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT gaggiottimonicadelcarmen enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT simonellilaura enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT marinicarlo enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT marinifederico enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT boadaroberto enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT lluganymerce enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT valientemanuel enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT ceccoligabriel enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT stoffelmariamicaela enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT viltresportalesmarcia enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT piccojuanmanuel enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT guevaramariagabriela enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy
AT munozfernandofelipe enhancingorganicseleniumformsinalfalfaforagethroughinorganicseleniumfoliarapplicationinsightsfromlaboratoryandfieldstudiesusingxrayspectroscopy