A comparison of the enzymatic properties of the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi

Congopain and cruzipain, the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi, were compared for their activities towards a series of new, sensitive fluorogenic substrates of the papain family of cysteine proteinases and for their sensitivity to inhibition by cystatins an...

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Autores principales: Chagas, J.R., Authié, Edith, Servean, C., Lalmanach, G., Juliano, L., Gauthier, F.
Formato: Journal Article
Lenguaje:Inglés
Publicado: Elsevier 1997
Materias:
Acceso en línea:https://hdl.handle.net/10568/33058
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author Chagas, J.R.
Authié, Edith
Servean, C.
Lalmanach, G.
Juliano, L.
Gauthier, F.
author_browse Authié, Edith
Chagas, J.R.
Gauthier, F.
Juliano, L.
Lalmanach, G.
Servean, C.
author_facet Chagas, J.R.
Authié, Edith
Servean, C.
Lalmanach, G.
Juliano, L.
Gauthier, F.
author_sort Chagas, J.R.
collection Repository of Agricultural Research Outputs (CGSpace)
description Congopain and cruzipain, the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi, were compared for their activities towards a series of new, sensitive fluorogenic substrates of the papain family of cysteine proteinases and for their sensitivity to inhibition by cystatins and related biotinylated peptidyl diazomethanes. Low K1 values, in the 10 pM range, were found for the interaction of both proteinases with natural cystatin inhibitors. The kinetic constants for the hydrolysis of cystatin-derived substrates, and the inhibition by related diazomethanes' were essentially identical. Unlike cathepsins B, and L, the related mammal papain family proteinases, congopain and cruzipain accomodate a prolyl residue in P2'. Substrates having the sequence VGGP from P2 to P2' were hydrolysed by both congopain and cruzipain with a K cat/Km greater than 4.10(3) mM-1 S-1. Irreversible diazomethane inhibitors, deduced from the unprime sequence of cystatin-derived substrates, inhibited the two parasite proteinases. N-terminal labelling of diazomethanes with a biotin group did not alter the rate of inhibitition significantly, which provides a useful tool for examining the distribution of these enzymes in the parasite and in the host. Despite their similar activities on cystatin-derived substrates, congopain and cruzipain had significantly different pH-activity profiles when assayed with a cystatin-derived substrate. They were correlated with structural differences, especially at the presumed S2 subsites.
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spelling CGSpace330582024-05-01T08:15:47Z A comparison of the enzymatic properties of the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi Chagas, J.R. Authié, Edith Servean, C. Lalmanach, G. Juliano, L. Gauthier, F. trypanosoma congolense trypanosoma cruzi cysteine enzymes enzyme inhibitors molecular biology parasitology Congopain and cruzipain, the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi, were compared for their activities towards a series of new, sensitive fluorogenic substrates of the papain family of cysteine proteinases and for their sensitivity to inhibition by cystatins and related biotinylated peptidyl diazomethanes. Low K1 values, in the 10 pM range, were found for the interaction of both proteinases with natural cystatin inhibitors. The kinetic constants for the hydrolysis of cystatin-derived substrates, and the inhibition by related diazomethanes' were essentially identical. Unlike cathepsins B, and L, the related mammal papain family proteinases, congopain and cruzipain accomodate a prolyl residue in P2'. Substrates having the sequence VGGP from P2 to P2' were hydrolysed by both congopain and cruzipain with a K cat/Km greater than 4.10(3) mM-1 S-1. Irreversible diazomethane inhibitors, deduced from the unprime sequence of cystatin-derived substrates, inhibited the two parasite proteinases. N-terminal labelling of diazomethanes with a biotin group did not alter the rate of inhibitition significantly, which provides a useful tool for examining the distribution of these enzymes in the parasite and in the host. Despite their similar activities on cystatin-derived substrates, congopain and cruzipain had significantly different pH-activity profiles when assayed with a cystatin-derived substrate. They were correlated with structural differences, especially at the presumed S2 subsites. 1997-09 2013-07-03T05:26:00Z 2013-07-03T05:26:00Z Journal Article https://hdl.handle.net/10568/33058 en Limited Access Elsevier Molecular and Biochemical Parasitology;88: 85-94
spellingShingle trypanosoma congolense
trypanosoma cruzi
cysteine
enzymes
enzyme inhibitors
molecular biology
parasitology
Chagas, J.R.
Authié, Edith
Servean, C.
Lalmanach, G.
Juliano, L.
Gauthier, F.
A comparison of the enzymatic properties of the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi
title A comparison of the enzymatic properties of the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi
title_full A comparison of the enzymatic properties of the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi
title_fullStr A comparison of the enzymatic properties of the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi
title_full_unstemmed A comparison of the enzymatic properties of the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi
title_short A comparison of the enzymatic properties of the major cysteine proteinases from Trypanosoma congolense and Trypanosoma cruzi
title_sort comparison of the enzymatic properties of the major cysteine proteinases from trypanosoma congolense and trypanosoma cruzi
topic trypanosoma congolense
trypanosoma cruzi
cysteine
enzymes
enzyme inhibitors
molecular biology
parasitology
url https://hdl.handle.net/10568/33058
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