Optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties

Pigmented paddy rice is rich in a diverse array of phytochemicals that confer notable antioxidant and anticancer properties. However, the stability and bioaccessibility of these bioactive compounds present significant challenges. In this study, 542 brown (including pigmented and non-pigmented) whole...

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Main Authors: Tiozon, Rhowell Navarro, Ong, Glenn Vincent P., Sartagoda, Kristel June D., Duque, Sheba Mae M., Alseekh, Saleh, Bonto, Aldrin P., Gempesaw, Shem, Pratap, Vipin, Reginio, Florencio C., Tengco, Jonina Marie J., Seagan, Christian, Tolentino, Joel H. G., Santiago, Dennis Marvin O., Fernie, Alisdair R., Sreenivasulu, Nese
Format: Journal Article
Language:Inglés
Published: Elsevier 2025
Subjects:
Online Access:https://hdl.handle.net/10568/175733
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author Tiozon, Rhowell Navarro
Ong, Glenn Vincent P.
Sartagoda, Kristel June D.
Duque, Sheba Mae M.
Alseekh, Saleh
Bonto, Aldrin P.
Gempesaw, Shem
Pratap, Vipin
Reginio, Florencio C.
Tengco, Jonina Marie J.
Seagan, Christian
Tolentino, Joel H. G.
Santiago, Dennis Marvin O.
Fernie, Alisdair R.
Sreenivasulu, Nese
author_browse Alseekh, Saleh
Bonto, Aldrin P.
Duque, Sheba Mae M.
Fernie, Alisdair R.
Gempesaw, Shem
Ong, Glenn Vincent P.
Pratap, Vipin
Reginio, Florencio C.
Santiago, Dennis Marvin O.
Sartagoda, Kristel June D.
Seagan, Christian
Sreenivasulu, Nese
Tengco, Jonina Marie J.
Tiozon, Rhowell Navarro
Tolentino, Joel H. G.
author_facet Tiozon, Rhowell Navarro
Ong, Glenn Vincent P.
Sartagoda, Kristel June D.
Duque, Sheba Mae M.
Alseekh, Saleh
Bonto, Aldrin P.
Gempesaw, Shem
Pratap, Vipin
Reginio, Florencio C.
Tengco, Jonina Marie J.
Seagan, Christian
Tolentino, Joel H. G.
Santiago, Dennis Marvin O.
Fernie, Alisdair R.
Sreenivasulu, Nese
author_sort Tiozon, Rhowell Navarro
collection Repository of Agricultural Research Outputs (CGSpace)
description Pigmented paddy rice is rich in a diverse array of phytochemicals that confer notable antioxidant and anticancer properties. However, the stability and bioaccessibility of these bioactive compounds present significant challenges. In this study, 542 brown (including pigmented and non-pigmented) whole grain rice samples were screened for their antioxidant components and capacity, leading to the identification of three superior cultivars: Balatinao variable purple rice, Ketan Hitam variable purple rice, and Kintuman red rice. Using response surface methodology, rice bran extracts from these cultivars were subjected to microencapsulation to stabilize the phytochemicals. Among the microencapsulated rice bran extracts (MRBEs), Ketan Hitam MRBE demonstrated significantly higher total phenolic content (TPC) and antioxidant capacity. This enhancement is likely due to the increased concentrations of isovitexin, luteolin 7-glucoside, and vitexin following microencapsulation. Furthermore, compared to non-encapsulated rice bran extracts, MRBEs exhibited significantly improved anticancer activity against HCT116 (colon) and A549 (lung) cancer cell lines (P < 0.05). Subsequent fractionation of the MRBE allowed for the identification of the most bioactive fractions, which contained metabolites effective against these cancer cell lines. In addition, in vitrobioaccessibility assays revealed a controlled release of 19 targeted phenolic compounds. This release profile was characterized by an initial increase during the gastric digestion phase, followed by a decrease in the intestinal phase. Notably, phenolic compounds such as chlorogenic acid, gallic acid, and vanillin were preserved across the three rice varieties after microencapsulation. These findings underscore the potential of MRBEs as functional food ingredients or supplements, offering improved bioaccessibility of phenolics, enhanced antioxidant properties, and promising anticancer activity. The results support the integration of rice bran extracts into the rice value chain, promoting their use in functional health applications.
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spelling CGSpace1757332025-12-23T01:44:18Z Optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties Tiozon, Rhowell Navarro Ong, Glenn Vincent P. Sartagoda, Kristel June D. Duque, Sheba Mae M. Alseekh, Saleh Bonto, Aldrin P. Gempesaw, Shem Pratap, Vipin Reginio, Florencio C. Tengco, Jonina Marie J. Seagan, Christian Tolentino, Joel H. G. Santiago, Dennis Marvin O. Fernie, Alisdair R. Sreenivasulu, Nese rice bran brown rice antioxidants phenolic compounds functional foods phytochemicals bioactive compounds food processing food composition food quality metabolites cell lines food supplements Pigmented paddy rice is rich in a diverse array of phytochemicals that confer notable antioxidant and anticancer properties. However, the stability and bioaccessibility of these bioactive compounds present significant challenges. In this study, 542 brown (including pigmented and non-pigmented) whole grain rice samples were screened for their antioxidant components and capacity, leading to the identification of three superior cultivars: Balatinao variable purple rice, Ketan Hitam variable purple rice, and Kintuman red rice. Using response surface methodology, rice bran extracts from these cultivars were subjected to microencapsulation to stabilize the phytochemicals. Among the microencapsulated rice bran extracts (MRBEs), Ketan Hitam MRBE demonstrated significantly higher total phenolic content (TPC) and antioxidant capacity. This enhancement is likely due to the increased concentrations of isovitexin, luteolin 7-glucoside, and vitexin following microencapsulation. Furthermore, compared to non-encapsulated rice bran extracts, MRBEs exhibited significantly improved anticancer activity against HCT116 (colon) and A549 (lung) cancer cell lines (P < 0.05). Subsequent fractionation of the MRBE allowed for the identification of the most bioactive fractions, which contained metabolites effective against these cancer cell lines. In addition, in vitrobioaccessibility assays revealed a controlled release of 19 targeted phenolic compounds. This release profile was characterized by an initial increase during the gastric digestion phase, followed by a decrease in the intestinal phase. Notably, phenolic compounds such as chlorogenic acid, gallic acid, and vanillin were preserved across the three rice varieties after microencapsulation. These findings underscore the potential of MRBEs as functional food ingredients or supplements, offering improved bioaccessibility of phenolics, enhanced antioxidant properties, and promising anticancer activity. The results support the integration of rice bran extracts into the rice value chain, promoting their use in functional health applications. 2025-06 2025-07-23T05:57:06Z 2025-07-23T05:57:06Z Journal Article https://hdl.handle.net/10568/175733 en Open Access application/pdf Elsevier Tiozon Jr, Rhowell Navarro, Glenn Vincent Ong, Kristel June D. Sartagoda, Sheba Mae M. Duque, Saleh Alseekh, Aldrin P. Bonto, Shem Gempesaw Jr et al. "Optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties." Food Hydrocolloids for Health (2025): 100221.
spellingShingle rice bran
brown rice
antioxidants
phenolic compounds
functional foods
phytochemicals
bioactive compounds
food processing
food composition
food quality
metabolites
cell lines
food supplements
Tiozon, Rhowell Navarro
Ong, Glenn Vincent P.
Sartagoda, Kristel June D.
Duque, Sheba Mae M.
Alseekh, Saleh
Bonto, Aldrin P.
Gempesaw, Shem
Pratap, Vipin
Reginio, Florencio C.
Tengco, Jonina Marie J.
Seagan, Christian
Tolentino, Joel H. G.
Santiago, Dennis Marvin O.
Fernie, Alisdair R.
Sreenivasulu, Nese
Optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties
title Optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties
title_full Optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties
title_fullStr Optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties
title_full_unstemmed Optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties
title_short Optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties
title_sort optimization of phenolic extraction method and in vitro bioaccessibility of microencapsulated pigmented rice bran extracts and their antioxidant and anticancer properties
topic rice bran
brown rice
antioxidants
phenolic compounds
functional foods
phytochemicals
bioactive compounds
food processing
food composition
food quality
metabolites
cell lines
food supplements
url https://hdl.handle.net/10568/175733
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