Antidiabetic and antioxidant profiling of 67 African trifoliate yam accessions by planar on-surface assays versus in vitro assays

Trifoliate yam (Dioscorea dumetorum) is traditionally used to treat diabetics in Nigeria. However, almost no information is available on its antidiabetic constituents and their natural variance. Hence, the activity of methanolic tuber extracts of 67 trifoliate yam accessions from the largest collect...

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Autores principales: Aiyedun, P.O., Sonibare, M.A., Gueye, B., Albach, D.C., Heil, J., Morlock, G.E.
Formato: Journal Article
Lenguaje:Inglés
Publicado: Elsevier 2025
Materias:
Acceso en línea:https://hdl.handle.net/10568/174510
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author Aiyedun, P.O.
Sonibare, M.A.
Gueye, B.
Albach, D.C.
Heil, J.
Morlock, G.E.
author_browse Aiyedun, P.O.
Albach, D.C.
Gueye, B.
Heil, J.
Morlock, G.E.
Sonibare, M.A.
author_facet Aiyedun, P.O.
Sonibare, M.A.
Gueye, B.
Albach, D.C.
Heil, J.
Morlock, G.E.
author_sort Aiyedun, P.O.
collection Repository of Agricultural Research Outputs (CGSpace)
description Trifoliate yam (Dioscorea dumetorum) is traditionally used to treat diabetics in Nigeria. However, almost no information is available on its antidiabetic constituents and their natural variance. Hence, the activity of methanolic tuber extracts of 67 trifoliate yam accessions from the largest collection in Africa was proven by four colorimetric antidiabetic and antioxidant in vitro assays, as diabetes is also linked with oxidative stress. For the first time, selected accessions were also analyzed by planar bioactivity profiling. It has a comparatively higher, more differentiated information content, is more sustainable in terms of material consumption, and enables straightforward compound prioritization and characterization. Up to a dozen individual antioxidant zones were revealed as well as one prominent zone inhibiting α-glucosidase and α-amylase. The latter inhibition zone was tentatively assigned to palmitic, linoleic, oleic, linolenic, oxo-nonanoic fatty acids by direct elution to heated electrospray ionization high-resolution mass spectrometry.
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spelling CGSpace1745102025-12-08T10:11:39Z Antidiabetic and antioxidant profiling of 67 African trifoliate yam accessions by planar on-surface assays versus in vitro assays Aiyedun, P.O. Sonibare, M.A. Gueye, B. Albach, D.C. Heil, J. Morlock, G.E. dioscorea bioactive properties chromatography Trifoliate yam (Dioscorea dumetorum) is traditionally used to treat diabetics in Nigeria. However, almost no information is available on its antidiabetic constituents and their natural variance. Hence, the activity of methanolic tuber extracts of 67 trifoliate yam accessions from the largest collection in Africa was proven by four colorimetric antidiabetic and antioxidant in vitro assays, as diabetes is also linked with oxidative stress. For the first time, selected accessions were also analyzed by planar bioactivity profiling. It has a comparatively higher, more differentiated information content, is more sustainable in terms of material consumption, and enables straightforward compound prioritization and characterization. Up to a dozen individual antioxidant zones were revealed as well as one prominent zone inhibiting α-glucosidase and α-amylase. The latter inhibition zone was tentatively assigned to palmitic, linoleic, oleic, linolenic, oxo-nonanoic fatty acids by direct elution to heated electrospray ionization high-resolution mass spectrometry. 2025-01 2025-05-09T09:55:04Z 2025-05-09T09:55:04Z Journal Article https://hdl.handle.net/10568/174510 en Open Access application/pdf Elsevier Aiyedun, P.O., Sonibare, M.A., Gueye, B., Albach, D.C., Heil, J. & Morlock, G.E. (2025). Antidiabetic and antioxidant profiling of 67 African trifoliate yam accessions by planar on-surface assays versus in vitro assays. Fitoterapia, 180: 106299, 1-12.
spellingShingle dioscorea
bioactive properties
chromatography
Aiyedun, P.O.
Sonibare, M.A.
Gueye, B.
Albach, D.C.
Heil, J.
Morlock, G.E.
Antidiabetic and antioxidant profiling of 67 African trifoliate yam accessions by planar on-surface assays versus in vitro assays
title Antidiabetic and antioxidant profiling of 67 African trifoliate yam accessions by planar on-surface assays versus in vitro assays
title_full Antidiabetic and antioxidant profiling of 67 African trifoliate yam accessions by planar on-surface assays versus in vitro assays
title_fullStr Antidiabetic and antioxidant profiling of 67 African trifoliate yam accessions by planar on-surface assays versus in vitro assays
title_full_unstemmed Antidiabetic and antioxidant profiling of 67 African trifoliate yam accessions by planar on-surface assays versus in vitro assays
title_short Antidiabetic and antioxidant profiling of 67 African trifoliate yam accessions by planar on-surface assays versus in vitro assays
title_sort antidiabetic and antioxidant profiling of 67 african trifoliate yam accessions by planar on surface assays versus in vitro assays
topic dioscorea
bioactive properties
chromatography
url https://hdl.handle.net/10568/174510
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